Save your unusable raws Guaranteed.

I'd i had lost that would definitely be the case but once I showed him he asked for a BTC wallet and gave me a refund.
least they helped you....these china men are ruthless sometimes. even after you had LONG TERM business. they would have gained more money off me doing the right thing then this cheap stupid 5k scam....
 
least they helped you....these china men are ruthless sometimes. even after you had LONG TERM business. they would have gained more money off me doing the right thing then this cheap stupid 5k scam....
It is all individual basis i have chinese suppliers i really trust and ones I don't. Most of the Indian companies are straight up scammers but I have one that refunded me 10k bucks because they had a couple seizures and he was afraid my product would get seized even though they have no reship policy and it would have been on me. Just like we have UGLs that build cleanrooms in their home and run sterility and pyrogen testing on every batch like a GMP facility and we have dudes that test nothing and fill unsterilized vials in their dirty kitchen with no gloves on. Integrity is hit or miss bro.
 
It is all individual basis i have chinese suppliers i really trust and ones I don't. Most of the Indian companies are straight up scammers but I have one that refunded me 10k bucks because they had a couple seizures and he was afraid my product would get seized even though they have no reship policy and it would have been on me. Just like we have UGLs that build cleanrooms in their home and run sterility and pyrogen testing on every batch like a GMP facility and we have dudes that test nothing and fill unsterilized vials in their dirty kitchen with no gloves on. Integrity is hit or miss bro.
the ass boogers doing it bare handed is NASTY lol GLOVES ARE MANIDTORY FOLKS (so is your hepa filter flow hood while we are at it)
 
the ass boogers doing it bare handed is NASTY lol GLOVES ARE MANIDTORY FOLKS (so is your hepa filter flow hood while we are at it)
A lot of that is ignorance. People learn the honebrew methods that are only acceptable if its personal use and then hey you're putting it in your body and thats on you. But the moment you brand it and sell it to people you need to hold yourself to a higher standard.
 
A lot of that is ignorance. People learn the honebrew methods that are only acceptable if its personal use and then hey you're putting it in your body and thats on you. But the moment you brand it and sell it to people you need to hold yourself to a higher standard.
100% iv spent so much in equipment in the long run that thats in the long run where my profits are but to know i wont kill or hurt anyone is a nice insurance. one bad death on my part and my life is over.
 
A lot of that is ignorance. People learn the honebrew methods that are only acceptable if its personal use and then hey you're putting it in your body and thats on you. But the moment you brand it and sell it to people you need to hold yourself to a higher standard.
i like your thinking man i can tell your a hidden gem, theres only one other guy i know who is like this @Venom Lab hes got the eu covered and likely will be the GO TO for someone who knows his stuff.
 
i will be posting jano hplc and gcms on pre starting raw test E shit ass india raws




and jano jplc gcms on THE AFTER (stand by and watch closely)

this will end this bullcrap narrative that it doesnt work


Then we can come together and play kumbaya

<3

lets start
1767973733569.webp
 
of course i would 95% is great dont waste your time unless its 90% pure thers a point where doing more is a waste now if you confirm these raws are weird and looking off id do it anyways. the more you have the better off you are doing it in mass. if i had raws 96% pure id consider it "good enough" it really depends on how much you have to lose or gain here. thats not to say i dont personally do better when i can because i do its my name after all. clear pharma. but 95% pure jano on raws you tested is good. over dose by 6% call it good. you will be within 8% on target which is still better than pharma. what people really want to see is your gcms and see if your oil is clean. as long as your better than pharma you wont have issues. im always always within 5% or better but thats just me and my standards . my recent purification was within 4% and the raws was ASS starting out. i call that a

of course i would 95% is great dont waste your time unless its 90% pure thers a point where doing more is a waste now if you confirm these raws are weird and looking off id do it anyways. the more you have the better off you are doing it in mass. if i had raws 96% pure id consider it "good enough" it really depends on how much you have to lose or gain here. thats not to say i dont personally do better when i can because i do its my name after all. clear pharma. but 95% pure jano on raws you tested is good. over dose by 6% call it good. you will be within 8% on target which is still better than pharma. what people really want to see is your gcms and see if your oil is clean. as long as your better than pharma you wont have issues. im always always within 5% or better but thats just me and my standards . my recent purification was within 4% and the raws was ASS starting out. i call that a win.

of course i would 95% is great dont waste your time unless its 90% pure thers a point where doing more is a waste now if you confirm these raws are weird and looking off id do it anyways. the more you have the better off you are doing it in mass. if i had raws 96% pure id consider it "good enough" it really depends on how much you have to lose or gain here. thats not to say i dont personally do better when i can because i do its my name after all. clear pharma. but 95% pure jano on raws you tested is good. over dose by 6% call it good. you will be within 8% on target which is still better than pharma. what people really want to see is your gcms and see if your oil is clean. as long as your better than pharma you wont have issues. im always always within 5% or better but thats just me and my standards . my recent purification was within 4% and the raws was ASS starting out. i call that a win.
I was happy with the way the raws looked. Snow white brick and chunks. Slight waxy feel. Dissolved easily between fingers. I appreciate your continued share of expertise man.
 

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Quick summary of my TRE journey.

Thank you @mongo5165 for keeping this thread alive.
If you do play with more raws please share.

(On a side note, i think there's a UGL lab in Spain that can test for solvents.)
 
Gravimetric drying after weigh a sample of the finished completely dry material and put that in a desicator or lab oven spread out at like 40°C and give it a day then reweigh the sample not a shitty 15 dollar scale you need a real 0.001 balance. If it lost weight you still have moisture present
 
Solvents are the least of your worries and extremely easy ro remove.
Iv said this from the start when I started this thread under scholar of brew. The solvents is the least of anyone's worries they are so easy to remove when using the right equipment. I got a lot of criticism in the past claiming fear-mongering that solvents were just going to stay in your raws even if you tried your hardest to remove them

I mean I get it but at the same time these solvents we use have a much lower boiling point than water lol. Acetone. Ethanol. These things are so easy to extract with a little bit of vacuuming. They don't just get trapped and stay stuck. Agitate vacuum rinse and repeat even overkill it 5 hours into a vacuum with a little bit of heat. Perfect solvent extraction.
 
Recrystallization is the last step in synthesis to clean up the final product if the raws are only 85% ypu really think worse solvents would already be present? They evaporate extremely easy its the co-soluble junk that stays behind.
 
As said by others surface solvents are easy to remove via vacuum and mild heat. But solvent/impurities can and will get trapped in the lattice and amorphous regions if crystals rapid form. This is why we are recrystallizing in the first place. Its the shit that gets trapped behind from yield being more important than quality. Just did recryst on some of the shit TC from AASraw I just got. Off to Jano Monday with before and after samples. MP is good at 101.2 initial and 102 clear. Nice sharp MP. Happy with the result on it. Just ethanol as solvent and carbon wash/filter through celite and slow cool from 60c. Seeded at 40c. MP video starts at 101c 1c/min rate. Out of the bag MP was 90c initial and 100c clear. So both depressed and extended. Powder looked fairly white(light beige)but was yellow as piss once in BB, would not go into dissolution. I ran it up to 250mg/ml in straight BB and up to 150c.
View attachment IMG_6521.mov
 
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