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[Motojager]

I'm assuming it's something insouble clogging the flters big time.
I would try filtering it via SS sieves.

Starting from 50um all the way down to 1um

I suggest just not purchasing it. You can run it through all the filters you want but the quinones / conjugated impurities will always be there. Unless you recryst. AASraw needs to just take control of the shit product they sent in these batches and make it right to the people that got any of these batches.

 

[Photon]

I suggest just not purchasing it. You can run it through all the filters you want but the quinones / conjugated impurities will always be there. Unless you recryst. AASraw needs to just take control of the shit product they sent in these batches and make it right to the people that got any of these batches.

Oh definitely.
At this point I'm probably not going to ever buy anything from them anymore..

83% TNE + 85% TRE and the only response I get is that Jano is not accurate is good enough a reason for me. Majority of the test results they've posted are nowhere close to any 3rd party test results either.

 

[RocketSurge0n]

Bottle Top Millipore

Everything is normal, even the filter is clean looking just slow.

My take is this batch was a fixed no melt batch, makes sense to me.

Was your powder a shade darker of white than usual?

Thank God the pump has it going and looks like I'll be fine but as others have reported, will take a bit longer.

I will just from this point on mix a little of the stuff with the other stuff I have each batch.

2000ml yesterday took 2.5hr of other stuff, 2000ml today I'm at 2hr and 1/3 of the way done. Today mixed almost half with the other stuff. So there is that as well!

The test 100ml I made to see if it would melt didn't crash, so that's another good sign, that didn't get filtered until yesterday when added to different raws.

I'll just stretch this stuff out for now on, but most don't have the luxury to do so.

I'm sure I'm a lot smaller than you as well, just private with faithfuls for 15 years that also refer others.

Are you using the disposable Milliopore bottle top filters?

 

[The-Squat]

Are you using the disposable Milliopore bottle top filters?

Yes, 500ml on a media bottle with electric pump

 

[RocketSurge0n]

Yes, 500ml on a media bottle with electric pump

Amazing. Thank you.

 

[Photon]

Correct plugged 250mg/ml into the steroidhomebrew calculator. Then added the cheeky 5% so was expecting 262.5

How many ml did you brew?
What did you filter it with?

262.5/0.917=286mg/ml

 

[Photon]

Yes 95%(BUT shit for those who dont follow) also did GCMS on it

This is..very interesting.
Let's say..we have 2 scenarios.

1.
Raws 95% purity, the remaining 5% dissolves, all soluble, filters fine.
I think this is the usual case scenario we have.

2.
Raws 95% purity, 5% doesn't dissolve, filters clog.
5% of a kilo is 50g.

a 33mm .22um syringe filter can only store about 10-20mg of junk.
a 100mm membrane filter? 150-200mg?

You can see that neither is going to filter it.
But isn't this a better scenario?

In a perfect scenario, all 5% gets filtered and you get a fully pure product.
And well, someone needs to adjust for displacement too

(am i missing something?)

 

[amicedrot]

This is..very interesting.
Let's say..we have 2 scenarios.

1.
Raws 95% purity, the remaining 5% dissolves, all soluble, filters fine.
I think this is the usual case scenario we have.

2.
Raws 95% purity, 5% doesn't dissolve, filters clog.
5% of a kilo is 50g.

a 33mm .22um syringe filter can only store about 10-20mg of junk.
a 100mm membrane filter? 150-200mg?

You can see that neither is going to filter it.
But isn't this a better scenario?

In a perfect scenario, all 5% gets filtered and you get a fully pure product.
And well, someone needs to adjust for displacement too

(am i missing something?)

i bet im missing way more than you are. but i am watching eagerly for the answer

 

[SuperJew]

I received 50g of Test E that is more compact than any I've seen in over 20 years. I'm thinking of sending it out to AB for testing. From what I'm gathering, breaking off a chunk isn't the best way to ensure accurate results. Is there a specific way I should break it down to try and maximize accuracy?

 

[IndividualMan]

I received 50g of Test E that is more compact than any I've seen in over 20 years. I'm thinking of sending it out to AB for testing. From what I'm gathering, breaking off a chunk isn't the best way to ensure accurate results. Is there a specific way I should break it down to try and maximize accuracy?

Blender or mortar and pestle

 

[Diesel77]

How many ml did you brew?
What did you filter it with?

262.5/0.917=286mg/ml

The brew was 260ml and vacuum filtered with .22 bottle top filter. I decap alk viles and fill them under a laminar flow hood.. I did small batch , basically just wanted to see if I had any issues with the raws fully dissolving.. I'm currently looking for a new filter set up. I can't find disposable ptfe bottle tops .all I see in .22bottle tops are pes or pvdf. I've been looking at glass vacuum assemblies that take the ptfe filter membranes. I have ptfe syringe filters but it's such a pain. I'm open to filter assembly suggestions. Share brew porn I love new lab ware