Save your unusable raws Guaranteed.

We can always add anhydrous magnesium sulfate as well ( purified dried Epson salts). I've done that and its dry as a bone. Just make sure you have a good filter stack with woven glass fiber filters on front end to take the bulk particles from the magnesium sulfate. Bottle tops aren't great for this because its easy to overload the membrane. Unless you guy the ones with the prefilter

This setup with the glass filters and 0.2 ptfe underneath worked best for me
FOUR E'S SCIENTIFIC Lab Vacuum Filtration Distillation Apparatus https://a.co/d/inuiX0b (Amazon.com)

Omicron Borosilicate Glass Fiber https://a.co/d/hKel0du (Amazon.com)

Dinglab 47mm,Hydrophobic PTFE Membrane Filter,Made by Polytetrafluoroethylene,50 Sheet/Pack (0.1um) https://a.co/d/05CDNNb (Dinglab 47mm,Hydrophobic PTFE Membrane Filter,Made by Polytetrafluoroethylene,50 Sheet/Pack (0.1um): Amazon.com: Industrial & Scientific)
 
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Quick update, this 10g batch of test e was done solely with 100% ethanol, no water. Turned out great. Beautiful waxy, pure white glass like chips. Stripped out all the original yellow color. After i hot filtered, i placed the solition in my 3d printer chamber at 60c, with high fan speeds to drive out a majority of the ethanol. It was a think syrup consistancy before putting in the fridge, then the freezer. Grains started to grow overnight. 24 hrs later, It went straight from the freezer into the vacuum chamer and dried for a few hours. I plan to chop it up more and continue to dehydrate. Preciously, hexane deff gave the other batch a polymorphic structure of hard white grains shown in my previous pictures for reference.
 

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Is it just me or he’s saying a lot without giving a step by step process and talking way too much instead of gettin to the point. I’ve worked with alot of testosterones and I didn’t even bother reading the first paragraph almost stopped when he said testosterone melts at room temperature, false. 2 right off the dome come to mind

Test cyp. 104C
Test prop 118C

I’ll give him the benefit of the doubt to prove me wrong
my ai fucked up the transcription i didnt think it would blow up like this xd i ended up framing walt poor walt.

ai fucked what walt salt

- walter

sorry man ai fucked up what i said i was stricly refering to impure test e being supressed depending on the impurities because hepatonic acid is liquid at room temp, so if its primilarly being in test enen or biggest impurity its going to supress the melting point. test e is gonna be like goo. test e is stable at room temperature but the impure test e he had.


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my ai fucked up the transcription i didnt think it would blow up like this xd i ended up framing walt poor walt.

ai fucked what walt salt

- walter

sorry man ai fucked up what i said i was stricly refering to impure test e being supressed depending on the impurities because hepatonic acid is liquid at room temp, so if its primilarly being in test enen or biggest impurity its going to supress the melting point. test e is gonna be like goo. test e is stable at room temperature but the impure test e he had.


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Thank you for the additional revisions. You guys and your GD AI.

Clint Eastwood Coffee GIF


Heptanoic acid MFers. Spelling.


Thanks dinfar and Walt.
 
Thank you for the additional revisions. You guys and your GD AI.

Clint Eastwood Coffee GIF


Heptanoic acid MFers. Spelling.


Thanks dinfar and Walt.
haha walt had nothing to do with it. he just send me like 8 voice messages i was like yup transcribition ai here we go.

i f8ck4d him up.

i rechecked this morning because he was like dude thats not what i said, and he said impure test e in the first voice messages. and im like damn lmao
 
I'll be honest with you. It really pisses me off that you guys have me banned because I can't fucking contribute I can't sit there like you guys are so far. I get I get your your whole Well, we can't have a source being I mean, come on.

At Walter:

None of us banned you Walt. If you can operate within the constraints the board owner sets, then bring it up with him about possible re-admission.

Thanks for taking the time to respond and your contributions with this thread. Very nice.
 
None of us banned you Walt. If you can operate within the constraints the board owner sets, then bring it up with him about possible re-admission.
i wrote something similar to him. apparently he was not using ugl to sell shrooms but did it in private groups not related to his ugl.

idk but ive sold "hard" drugs while being a member in here but certainly not doing it online or meso or source related.

same with hyb slanging fent on the side, as long as they dont do it on here or their "hyb" account its not a problem.

i told his ass to bring proof and use contact us to try to get reinstated
 
haha walt had nothing to do with it. he just send me like 8 voice messages i was like yup transcribition ai here we go.

i f8ck4d him up.

i rechecked this morning because he was like dude thats not what i said, and he said impure test e in the first voice messages. and im like damn lmao

He keeps typing hepatonic acid and it is pissing me off, haha.
 
i wrote something similar to him. apparently he was not using ugl to sell shrooms but did it in private groups not related to his ugl.

idk but ive sold "hard" drugs while being a member in here but certainly not doing it online or meso or source related.

same with hyb slanging fent on the side, as long as they dont do it on here or their "hyb" account its not a problem.

i told his ass to bring proof and use contact us to try to get reinstated
That is correct, one or more members (sources?) here ratted out his other channels/"hobbies", etc.

I am just bringing up the obvious with respect to his ban. This thread and its contributions are a poster child for harm reduction and moving the community forward, especially in times like these.

And yes I hope he has [is] cleaned [cleaning] up his act. I don't want him to encounter any legal trouble.
 
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For scooping and scraping dried raws, these things are nearly invaluable. I hate the price but if you turn the spoon upside down, convex and scrape, you can get in every little corner...

LevGo® 17211 Standard smartSpatula® Disposable Multipurpose Laboratory Spatula, PP, 210 x 7 mm (300 spatulas per Pack). Look for The V at The Neck.® Amazon.com
 
For scooping and scraping dried raws, these things are nearly invaluable. I hate the price but if you turn the spoon upside down, convex and scrape, you can get in every little corner...

LevGo® 17211 Standard smartSpatula® Disposable Multipurpose Laboratory Spatula, PP, 210 x 7 mm (300 spatulas per Pack). Look for The V at The Neck.® Amazon.com
In my day with other crystalized material we used a slurpee straw :D :D looks about the same
 
@readalot @dinfar1337 whats your guys thoughts about proactivly treating test e raws for Heptanoic acid (or however you spell it) contamination after recrystalization when they are still cold? I was thinking washing with a usp sodium bicarbonate or sodium hydroxide sterile water solution, mixed to a pH of 8-9. Then rewashing with cold sterile water to wash everything away. Let me know what you think. Maybe line the raws bowl with a 300mesh nylon fabric, that way I could just pick the bag right out of the bowl.
 
Quick update, so using water as an anti-solvent was a failure. It should work but as you add more water to decrease solubility, it raises the freezing point, so it hard to get the testosterone to drop out of solution. When you put it into the freezer, it just forms into a giant iceball. Maybe less water, more ethanol would work but I dont think its worth it. There should be about 10grams of drop out in that media bottle and its deff way less than that. Time too add some molecular sieves to dry out the solution and try again with straight ethanol...

I have a 10g batch in the freezer now with ethyl acetate as the solvent and n-heptane as the anti-solvent. We will see in the next day how that one turns out.
 

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So this is the Test E /acetone batch. 10.1g to start and 8.7g recovered. There was some yellowing in the acetone crystals, probably oils . Once the acetone was dried off in the vacuum chamber, i redisolved the crystals in n-hexane. This seems to have reduced or eliminated the yellowing. Hexane was dobbed off after 24hrs in the freezer and redried. I plan to grind these down more and throw them back in the vacuum chamber
 

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That is correct, one or more members (sources?) here ratted out his other channels/"hobbies", etc.

I am just bringing up the obvious with respect to his ban. This thread and its contributions are a poster child for harm reduction and moving the community forward, especially in times like these.

And yes I hope he has [is] cleaned [cleaning] up his act. I don't want him to encounter any legal trouble.
He isn't, he was selling off pounds of mushrooms just last week and tweaking out of his skull
 

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