Small air bubbles in Test-Ent home brew

snuff-sann

New Member
Hya,

2 weeks ago I made 40ml of testosterone entanthate home-brew.
Everything went very smooth and I now have some nice test.
But when I saw the vial today it looked as if the test wasn't really clear anymore.
When I had a better look I saw a lot of very small air bubbles. Because of those small bubbles the oil looks a bit misty.
Do Ihave to worry now?
Is it still allright to use?
Is it because there isn't enough solvent in it and that the oil is a bit thicker.?
I allready used it last week and everything went fine.
Can anybody give me some info please?
 
I read a view topics here at Meso.
When you put your home-brew in the oven, do you have to stick a needle in the lid-rubber?
I have a feeling that the reason why it's a bit cloudy is because there's a bit a water in it cause when I put it in the oven I had no needle in it so the condens inside the vial couldn't get out.
Do you guys think that this could be the problem?
Can I fix it by re-heating it again and stich a needle in the rubber?
 
Just so you know it won't hurt you to shoot it as is but the only way to clear it up it to POP the top off do not insert pins condensation can not escape through a needle. When lid is all the way off you need to put it in a pan with no water in it and heat it to 300*F for 15 mins constantly monitor the heat it will be going up and down but attempt to keep it steady. When 15 is up do not remove the test from pan or it will explode out the top let it cool in pan for 30min. Set it in a cool dark place "room temp" and leave it alone for 2 hours after that check and see what she looks like it should be clear if not repeat untill clear. Keep in mind you will need some extra whatman filters and a sterial vile to put new product in good luck
 
Did you put test powder into oil as onle of the last steps. I'm trying to identify what conversion method you used.

I first put 10 grams of test-e powder in a glass beaker, then 2ml of BA, followed by 6ml of BB and finally 22ml of grapeseed-oil. After filtering it I used another 4ml of oil to get all of the test out of the filter.
But I have a feeling that I needed to put a needle in the vial-rubber when I was baking it in the oven. I didn't so condens in the vial couldn't get out and stayed in with the oil.
Is it correct that you need to put a needle into the vial-rubber when heating it into the oven?
 
Just so you know it won't hurt you to shoot it as is but the only way to clear it up it to POP the top off do not insert pins condensation can not escape through a needle. When lid is all the way off you need to put it in a pan with no water in it and heat it to 300*F for 15 mins constantly monitor the heat it will be going up and down but attempt to keep it steady. When 15 is up do not remove the test from pan or it will explode out the top let it cool in pan for 30min. Set it in a cool dark place "room temp" and leave it alone for 2 hours after that check and see what she looks like it should be clear if not repeat untill clear. Keep in mind you will need some extra whatman filters and a sterial vile to put new product in good luck

So you say that I can use it?

I used a closed sterile vial by the way.
I read in another topic that sticking a needle in will get rid of the condens when reheating it again.
 
The instructions I gave you were to clear test that may have been wet. But if your powder was dry and you heated Ba and bb solution withought venting it it may have built up pressure in this case just pin the top now and all presure will be released but that would have nothing to do with the cloudy test. Try my initial instructions and see what happens. Cloudy and bubbles is two differant things and look two differant ways so is it cloudy or is there bubbles? And are the bubbles there if you don't shake the test.
 
The instructions I gave you were to clear test that may have been wet. But if your powder was dry and you heated Ba and bb solution withought venting it it may have built up pressure in this case just pin the top now and all presure will be released but that would have nothing to do with the cloudy test. Try my initial instructions and see what happens. Cloudy and bubbles is two differant things and look two differant ways so is it cloudy or is there bubbles? And are the bubbles there if you don't shake the test.

But doesn't it get cloudy cause there's some water into the oil?
After heating it I could see some condens inside the vial, hanging against the vial above the oil. The oil was very clear. Now it looks like the water is mixed with the oil. I'm not really sure if its cloudy cause of the small bubbles or of the condens inside.
 
Ok on your last post you defined it as water. People will say pin it and heat it but try that it will NOT work water will just hit the pin and drip back. You need another sterial vile and a couple micro filters follow my steps above and your golden I just finished mine with the same problem and I tried to short cut it by putting 4 16G pinz in top you would think that's enough for the water to escape but it's not. Do it right if your goin to do it. If you choose to not clear it just heat it everytime befor shots so it's clear then pin it. I personally pinned 2weeks of cloudy test with no problem my opinion is it's just ugly and not contaminated
 
Ok on your last post you defined it as water. People will say pin it and heat it but try that it will NOT work water will just hit the pin and drip back. You need another sterial vile and a couple micro filters follow my steps above and your golden I just finished mine with the same problem and I tried to short cut it by putting 4 16G pinz in top you would think that's enough for the water to escape but it's not. Do it right if your goin to do it. If you choose to not clear it just heat it everytime befor shots so it's clear then pin it. I personally pinned 2weeks of cloudy test with no problem my opinion is it's just ugly and not contaminated

I know for sure it's sterile, I worked very clean.
So it's usable?

I'm going to make some more vials in 2 days. Do I need to put a needle into the vial-rubber when I'm heating it in the oven?
 
Yea don't worry. Think bout it if it's water and you were sterial how will water hurt you and by the way it takes 2 drops to cause 65ml of test to cloud. So chances Are you hardly have any water in it at all. If you are concerned then use my steps to clear but I personally would not mind using it I have all the supplies needed at house so I would clear it but still i wouldn't worry. O and if your scared of infection just heat your solution to 170* F to kill bacteria also that is why you put bb and ba into solution it helps steralize solution. Final verdict your fine don't worry in a perfect world you should clear it but don't worry it's fine the way it is
 
Thnx buddy, I will reheat it and see what happens, if it's gonna be all clear I will use it. When it has been cooled down ofcourse.
 
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